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The Literature of Classical Microchemistry, Spot Tests, and Chemical Microscopy
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John Gustav Delly, Scientific Advisor, College of Microscopy, Westmont, IL |
The 1940's
Most of the books written during the
World War 2 years were published after the war. Belcher and Wilson authored Qualitative
Inorganic Microanalysis [Belcher, R. and C.L. Wilson (1946)], in 1946. Ten
years later the second edition came out under the title, Inorganic
Microanalysis; Qualitative and Quantitative [Belcher, R. and C.L. Wilson
(1957)]. Many of the Emich-Schneider/Benedetti-Pichler/Chamot and Mason
techniques and apparatus are utilized here.
The year 1946 also saw the first edition
of Frank L. Schneider's Organic Qualitative Analysis [Schneider, F.L.
(1946)], which we will see again in 1964 as the much enlarged, Qualitative
Organic Microanalysis [Schneider, Frank L. (1964)].
The book, Reagents for Qualitative
Inorganic Analysis (1948) reports on new analytical reactions and
reagents (Figure 50).
M.N. Short’s
book on the Microscopic Determination of the Ore Minerals (Figure 51),
published in the previous decade, came out as a second edition in 1940 [Short
(1940)]. This volume contains a section on microchemical methods, and Figure
52 is one of the color photomicrographs illustrating a microchemical test for
silver.
Also in 1948, Kofler and Kofler's Mikromethoden
zur Kennzeichnung organischer Stoffe and Stoffgemische [Kofler, L. and Adelheid Kofler (1948)], was
issued. An English translation of
this book was made by McCrone in 1952, and
was, at one time, available from the McCrone Research Institute.
click image to enlarge (87K)
Figure
50. Title page of Reagents for Qualitative
Inorganic Analysis (1948).
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click image to enlarge (58K)
Figure
51. Title page of Short’s Microscopic
Determination of the Ore Minerals, Second Edition (1940). |
click image to enlarge (190K)
Figure
52. Photomicrographs of a microchemical test for silver in
Short’s Microscopic Determination of the
Ore Minerals, Second
Edition (1940). |
The 1950's
In 1950 there was a second printing of Benedetti-Pichler's Introduction to the Microtechnique of Inorganic
Analysis [Benedetti-Pichler, A.A.
(1942 and1950)]. In 1954 there appeared another edition of
Feigl's Spot Tests... [Feigl, Fritz and
Vinzenz Anger (1937, 1939, 1946, 1954, 1958)], [Feigl, Fritz (1937, 1939, 1946,
1954, 1956, 1960)], Maljaroff's
Qualitative anorganische Mikroanalyse [Maljaroff, K.L. (1953 and 1954)], first
published in 1953, went into a
second edition the following year.
Harold F. Schaeffer's very popular Microscopy For Chemists [Schaeffer, Harold F. (1953)], was
published in 1953. It is a
splendid book that went out of print, but demand for it remained sufficiently
high, and Dover reprinted it. And now the Dover reprint (Figure 53) is no
longer available. The
experiments in this book make it an excellent teach-yourself choice.
Alimarin and Archangelskaja's Qualitative Halbmikroanalyse [Alimarin,
I.P. and W.N. Archangelskaja (1956)], was published in 1956.
And in 1958 Malissa
and Benedetti-Pichler's Anorganische
qualitative Mikroanalyse [Malissa,
H. and A.A. Benedetti-Pichler (1958)], was published.
click image to enlarge (142K)
Figure
53. Front cover of the Dover reprint of Schaeffer’s
Microscopy for Chemistry (1953). |
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